Superconductivity and crystal structure of the palladium-iron-arsenides Ca10(Fe1-xPdxAs)10Pd3As8
Identifieur interne : 000446 ( Main/Repository ); précédent : 000445; suivant : 000447Superconductivity and crystal structure of the palladium-iron-arsenides Ca10(Fe1-xPdxAs)10Pd3As8
Auteurs : RBID : Pascal:13-0311648Descripteurs français
- Pascal (Inist)
- Supraconductivité, Structure cristalline, Palladium, Fer, Arséniure, Diffraction RX, Cristal triclinique, Groupe espace, Platine, Arsenic, Dimère, Symétrie cristalline, Propriété symétrie, Mode empilement, Etat solide, Réseau triclinique, Conductivité électrique, Addition lanthane, Transition supraconductrice, Addition fer, Spectrométrie Mössbauer, Effet Mössbauer, Ordre magnétique, Structure électronique, Forme cylindrique, Surface Fermi, Couche active, Température critique, Point critique, Addition indium, FeAs, 6166, 6150A.
- Wicri :
English descriptors
- KwdEn :
- Active layer, Arsenic, Arsenides, Critical points, Critical temperature, Crystal structure, Crystal symmetry, Cylindrical shape, Dimers, Electrical conductivity, Electronic structure, Fermi surface, Indium additions, Iron, Iron additions, Lanthanum additions, Magnetic ordering, Moessbauer effect, Moessbauer spectroscopy, Palladium, Platinum, Solid state, Space groups, Stacking sequence, Superconducting transitions, Superconductivity, Symmetry property, Triclinic crystals, Triclinic lattices, XRD.
Abstract
The palladium-iron-arsenides Ca10(Fe1-xPdxAs)10(Pd3As8) were synthesized by solid-state methods and characterized by X-ray powder and single crystal diffraction. The triclinic crystal structure (space group P1) is isotypic to the homologue platinum 1038-type superconductors with alternating FeAs4/4- and Pd3Asg-layers, each separated by layers of calcium atoms. Iron is tetrahedrally and palladium is planar coordinated by four arsenic atoms. As2-dimers (dAs-As ≃ 250 pm) are present in the Pd3As8-layer. Even though each layer itself has a four-fold rotational symmetry, the shifted layer stacking causes the triclinic space group. Resistivity measurements of La-doped samples show the onset of superconductivity at 17 K and zero resistivity below 10 K. The magnetic shielding fraction is about 20% at 3.5 K. 57Fe-Mössbauer spectra exhibit one absorption line and show no hint to magnetic ordering. The electronic structure is very similar to the known iron-arsenides with cylinder-like Fermi surfaces and partial nesting between hole- and electron-like sheets. Our results show that superconductivity in the palladium-iron-compounds is present but complicated by too high substitution of iron by palladium in the active FeAs-layers. Since the electronic preconditions are satisfied, we expect higher critical temperatures in Pd1038-compounds with lower or even without Pd-doping in the FeAs-layer.
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<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en" level="a">Superconductivity and crystal structure of the palladium-iron-arsenides Ca<sub>10</sub>(Fe<sub>1-x</sub>Pd<sub>x</sub>As)<sub>10</sub>Pd<sub>3</sub>As<sub>8</sub></title><author><name sortKey="Hieke, C" uniqKey="Hieke C">C. Hieke</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>Department Chemie der Ludwig-Maximilians-Universität, Butenandtstr. 5-13 (Haus D)</s1><s2>81377, München</s2><s3>DEU</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>8 aut.</sZ></inist:fA14><country>Allemagne</country><placeName><region type="land" nuts="1">Bavière</region><region type="district" nuts="2">District de Haute-Bavière</region><settlement type="city">Munich</settlement></placeName></affiliation></author><author><name sortKey="Lippmann, J" uniqKey="Lippmann J">J. Lippmann</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>Department Chemie der Ludwig-Maximilians-Universität, Butenandtstr. 5-13 (Haus D)</s1><s2>81377, München</s2><s3>DEU</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>8 aut.</sZ></inist:fA14><country>Allemagne</country><placeName><region type="land" nuts="1">Bavière</region><region type="district" nuts="2">District de Haute-Bavière</region><settlement type="city">Munich</settlement></placeName></affiliation></author><author><name sortKey="St Rzer, T" uniqKey="St Rzer T">T. St Rzer</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>Department Chemie der Ludwig-Maximilians-Universität, Butenandtstr. 5-13 (Haus D)</s1><s2>81377, München</s2><s3>DEU</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>8 aut.</sZ></inist:fA14><country>Allemagne</country><placeName><region type="land" nuts="1">Bavière</region><region type="district" nuts="2">District de Haute-Bavière</region><settlement type="city">Munich</settlement></placeName></affiliation></author><author><name sortKey="Friederichs, G" uniqKey="Friederichs G">G. Friederichs</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>Department Chemie der Ludwig-Maximilians-Universität, Butenandtstr. 5-13 (Haus D)</s1><s2>81377, München</s2><s3>DEU</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>8 aut.</sZ></inist:fA14><country>Allemagne</country><placeName><region type="land" nuts="1">Bavière</region><region type="district" nuts="2">District de Haute-Bavière</region><settlement type="city">Munich</settlement></placeName></affiliation></author><author><name sortKey="Nitsche, F" uniqKey="Nitsche F">F. Nitsche</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>Department Chemie der Ludwig-Maximilians-Universität, Butenandtstr. 5-13 (Haus D)</s1><s2>81377, München</s2><s3>DEU</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>8 aut.</sZ></inist:fA14><country>Allemagne</country><placeName><region type="land" nuts="1">Bavière</region><region type="district" nuts="2">District de Haute-Bavière</region><settlement type="city">Munich</settlement></placeName></affiliation></author><author><name sortKey="Winter, F" uniqKey="Winter F">F. Winter</name><affiliation wicri:level="1"><inist:fA14 i1="02"><s1>Institut für Anorganische und Analytische Chemie, Universität Münster, Corrensstr. 30</s1><s2>48149, Münster</s2><s3>DEU</s3><sZ>6 aut.</sZ><sZ>7 aut.</sZ></inist:fA14><country>Allemagne</country><wicri:noRegion>48149, Münster</wicri:noRegion><wicri:noRegion>Corrensstr. 30</wicri:noRegion><wicri:noRegion>48149, Münster</wicri:noRegion></affiliation></author><author><name sortKey="Pottgen, R" uniqKey="Pottgen R">R. Pöttgen</name><affiliation wicri:level="1"><inist:fA14 i1="02"><s1>Institut für Anorganische und Analytische Chemie, Universität Münster, Corrensstr. 30</s1><s2>48149, Münster</s2><s3>DEU</s3><sZ>6 aut.</sZ><sZ>7 aut.</sZ></inist:fA14><country>Allemagne</country><wicri:noRegion>48149, Münster</wicri:noRegion><wicri:noRegion>Corrensstr. 30</wicri:noRegion><wicri:noRegion>48149, Münster</wicri:noRegion></affiliation></author><author><name sortKey="Johrendt, D" uniqKey="Johrendt D">D. Johrendt</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>Department Chemie der Ludwig-Maximilians-Universität, Butenandtstr. 5-13 (Haus D)</s1><s2>81377, München</s2><s3>DEU</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>8 aut.</sZ></inist:fA14><country>Allemagne</country><placeName><region type="land" nuts="1">Bavière</region><region type="district" nuts="2">District de Haute-Bavière</region><settlement type="city">Munich</settlement></placeName></affiliation></author></titleStmt><publicationStmt><idno type="inist">13-0311648</idno><date when="2013">2013</date><idno type="stanalyst">PASCAL 13-0311648 INIST</idno><idno type="RBID">Pascal:13-0311648</idno><idno type="wicri:Area/Main/Corpus">000693</idno><idno type="wicri:Area/Main/Repository">000446</idno></publicationStmt><seriesStmt><idno type="ISSN">1478-6435</idno><title level="j" type="abbreviated">Philos. mag. : (2003, Print)</title><title level="j" type="main">Philosophical magazine : (2003. Print)</title></seriesStmt></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Active layer</term><term>Arsenic</term><term>Arsenides</term><term>Critical points</term><term>Critical temperature</term><term>Crystal structure</term><term>Crystal symmetry</term><term>Cylindrical shape</term><term>Dimers</term><term>Electrical conductivity</term><term>Electronic structure</term><term>Fermi surface</term><term>Indium additions</term><term>Iron</term><term>Iron additions</term><term>Lanthanum additions</term><term>Magnetic ordering</term><term>Moessbauer effect</term><term>Moessbauer spectroscopy</term><term>Palladium</term><term>Platinum</term><term>Solid state</term><term>Space groups</term><term>Stacking sequence</term><term>Superconducting transitions</term><term>Superconductivity</term><term>Symmetry property</term><term>Triclinic crystals</term><term>Triclinic lattices</term><term>XRD</term></keywords><keywords scheme="Pascal" xml:lang="fr"><term>Supraconductivité</term><term>Structure cristalline</term><term>Palladium</term><term>Fer</term><term>Arséniure</term><term>Diffraction RX</term><term>Cristal triclinique</term><term>Groupe espace</term><term>Platine</term><term>Arsenic</term><term>Dimère</term><term>Symétrie cristalline</term><term>Propriété symétrie</term><term>Mode empilement</term><term>Etat solide</term><term>Réseau triclinique</term><term>Conductivité électrique</term><term>Addition lanthane</term><term>Transition supraconductrice</term><term>Addition fer</term><term>Spectrométrie Mössbauer</term><term>Effet Mössbauer</term><term>Ordre magnétique</term><term>Structure électronique</term><term>Forme cylindrique</term><term>Surface Fermi</term><term>Couche active</term><term>Température critique</term><term>Point critique</term><term>Addition indium</term><term>FeAs</term><term>6166</term><term>6150A</term></keywords><keywords scheme="Wicri" type="concept" xml:lang="fr"><term>Fer</term><term>Platine</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">The palladium-iron-arsenides Ca<sub>10</sub>(Fe<sub>1-x</sub>Pd<sub>x</sub>As)<sub>10</sub>(Pd<sub>3</sub>As<sub>8</sub>) were synthesized by solid-state methods and characterized by X-ray powder and single crystal diffraction. The triclinic crystal structure (space group P1) is isotypic to the homologue platinum 1038-type superconductors with alternating FeAs<sub>4/4</sub>- and Pd<sub>3</sub>Asg-layers, each separated by layers of calcium atoms. Iron is tetrahedrally and palladium is planar coordinated by four arsenic atoms. As<sub>2</sub>-dimers (d<sub>As-As</sub> ≃ 250 pm) are present in the Pd<sub>3</sub>As<sub>8</sub>-layer. Even though each layer itself has a four-fold rotational symmetry, the shifted layer stacking causes the triclinic space group. Resistivity measurements of La-doped samples show the onset of superconductivity at 17 K and zero resistivity below 10 K. The magnetic shielding fraction is about 20% at 3.5 K. <sup>57</sup>Fe-Mössbauer spectra exhibit one absorption line and show no hint to magnetic ordering. The electronic structure is very similar to the known iron-arsenides with cylinder-like Fermi surfaces and partial nesting between hole- and electron-like sheets. Our results show that superconductivity in the palladium-iron-compounds is present but complicated by too high substitution of iron by palladium in the active FeAs-layers. Since the electronic preconditions are satisfied, we expect higher critical temperatures in Pd1038-compounds with lower or even without Pd-doping in the FeAs-layer.</div></front></TEI><inist><standard h6="B"><pA><fA01 i1="01" i2="1"><s0>1478-6435</s0></fA01><fA03 i2="1"><s0>Philos. mag. : (2003, Print)</s0></fA03><fA05><s2>93</s2></fA05><fA06><s2>25-27</s2></fA06><fA08 i1="01" i2="1" l="ENG"><s1>Superconductivity and crystal structure of the palladium-iron-arsenides Ca<sub>10</sub>(Fe<sub>1-x</sub>Pd<sub>x</sub>As)<sub>10</sub>Pd<sub>3</sub>As<sub>8</sub></s1></fA08><fA11 i1="01" i2="1"><s1>HIEKE (C.)</s1></fA11><fA11 i1="02" i2="1"><s1>LIPPMANN (J.)</s1></fA11><fA11 i1="03" i2="1"><s1>STÜRZER (T.)</s1></fA11><fA11 i1="04" i2="1"><s1>FRIEDERICHS (G.)</s1></fA11><fA11 i1="05" i2="1"><s1>NITSCHE (F.)</s1></fA11><fA11 i1="06" i2="1"><s1>WINTER (F.)</s1></fA11><fA11 i1="07" i2="1"><s1>PÖTTGEN (R.)</s1></fA11><fA11 i1="08" i2="1"><s1>JOHRENDT (D.)</s1></fA11><fA14 i1="01"><s1>Department Chemie der Ludwig-Maximilians-Universität, Butenandtstr. 5-13 (Haus D)</s1><s2>81377, München</s2><s3>DEU</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>8 aut.</sZ></fA14><fA14 i1="02"><s1>Institut für Anorganische und Analytische Chemie, Universität Münster, Corrensstr. 30</s1><s2>48149, Münster</s2><s3>DEU</s3><sZ>6 aut.</sZ><sZ>7 aut.</sZ></fA14><fA20><s1>3680-3689</s1></fA20><fA21><s1>2013</s1></fA21><fA23 i1="01"><s0>ENG</s0></fA23><fA43 i1="01"><s1>INIST</s1><s2>134A3</s2><s5>354000505832370190</s5></fA43><fA44><s0>0000</s0><s1>© 2013 INIST-CNRS. All rights reserved.</s1></fA44><fA45><s0>34 ref.</s0></fA45><fA47 i1="01" i2="1"><s0>13-0311648</s0></fA47><fA60><s1>P</s1></fA60><fA61><s0>A</s0></fA61><fA64 i1="01" i2="1"><s0>Philosophical magazine : (2003. Print)</s0></fA64><fA66 i1="01"><s0>GBR</s0></fA66><fC01 i1="01" l="ENG"><s0>The palladium-iron-arsenides Ca<sub>10</sub>(Fe<sub>1-x</sub>Pd<sub>x</sub>As)<sub>10</sub>(Pd<sub>3</sub>As<sub>8</sub>) were synthesized by solid-state methods and characterized by X-ray powder and single crystal diffraction. The triclinic crystal structure (space group P1) is isotypic to the homologue platinum 1038-type superconductors with alternating FeAs<sub>4/4</sub>- and Pd<sub>3</sub>Asg-layers, each separated by layers of calcium atoms. Iron is tetrahedrally and palladium is planar coordinated by four arsenic atoms. As<sub>2</sub>-dimers (d<sub>As-As</sub> ≃ 250 pm) are present in the Pd<sub>3</sub>As<sub>8</sub>-layer. Even though each layer itself has a four-fold rotational symmetry, the shifted layer stacking causes the triclinic space group. Resistivity measurements of La-doped samples show the onset of superconductivity at 17 K and zero resistivity below 10 K. The magnetic shielding fraction is about 20% at 3.5 K. <sup>57</sup>Fe-Mössbauer spectra exhibit one absorption line and show no hint to magnetic ordering. The electronic structure is very similar to the known iron-arsenides with cylinder-like Fermi surfaces and partial nesting between hole- and electron-like sheets. Our results show that superconductivity in the palladium-iron-compounds is present but complicated by too high substitution of iron by palladium in the active FeAs-layers. Since the electronic preconditions are satisfied, we expect higher critical temperatures in Pd1038-compounds with lower or even without Pd-doping in the FeAs-layer.</s0></fC01><fC02 i1="01" i2="3"><s0>001B60A66</s0></fC02><fC02 i1="02" i2="3"><s0>001B60A50A</s0></fC02><fC03 i1="01" i2="3" l="FRE"><s0>Supraconductivité</s0><s5>01</s5></fC03><fC03 i1="01" i2="3" l="ENG"><s0>Superconductivity</s0><s5>01</s5></fC03><fC03 i1="02" i2="3" l="FRE"><s0>Structure cristalline</s0><s5>02</s5></fC03><fC03 i1="02" i2="3" l="ENG"><s0>Crystal structure</s0><s5>02</s5></fC03><fC03 i1="03" i2="3" l="FRE"><s0>Palladium</s0><s2>NC</s2><s5>03</s5></fC03><fC03 i1="03" i2="3" l="ENG"><s0>Palladium</s0><s2>NC</s2><s5>03</s5></fC03><fC03 i1="04" i2="3" l="FRE"><s0>Fer</s0><s2>NC</s2><s5>04</s5></fC03><fC03 i1="04" i2="3" l="ENG"><s0>Iron</s0><s2>NC</s2><s5>04</s5></fC03><fC03 i1="05" i2="3" l="FRE"><s0>Arséniure</s0><s2>NA</s2><s5>05</s5></fC03><fC03 i1="05" i2="3" 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i1="17" i2="3" l="ENG"><s0>Electrical conductivity</s0><s5>29</s5></fC03><fC03 i1="18" i2="3" l="FRE"><s0>Addition lanthane</s0><s5>30</s5></fC03><fC03 i1="18" i2="3" l="ENG"><s0>Lanthanum additions</s0><s5>30</s5></fC03><fC03 i1="19" i2="3" l="FRE"><s0>Transition supraconductrice</s0><s5>31</s5></fC03><fC03 i1="19" i2="3" l="ENG"><s0>Superconducting transitions</s0><s5>31</s5></fC03><fC03 i1="20" i2="3" l="FRE"><s0>Addition fer</s0><s5>32</s5></fC03><fC03 i1="20" i2="3" l="ENG"><s0>Iron additions</s0><s5>32</s5></fC03><fC03 i1="21" i2="3" l="FRE"><s0>Spectrométrie Mössbauer</s0><s5>33</s5></fC03><fC03 i1="21" i2="3" l="ENG"><s0>Moessbauer spectroscopy</s0><s5>33</s5></fC03><fC03 i1="22" i2="3" l="FRE"><s0>Effet Mössbauer</s0><s5>34</s5></fC03><fC03 i1="22" i2="3" l="ENG"><s0>Moessbauer effect</s0><s5>34</s5></fC03><fC03 i1="23" i2="3" l="FRE"><s0>Ordre magnétique</s0><s5>35</s5></fC03><fC03 i1="23" i2="3" l="ENG"><s0>Magnetic ordering</s0><s5>35</s5></fC03><fC03 i1="24" i2="3" 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i2="3" l="FRE"><s0>Addition indium</s0><s5>42</s5></fC03><fC03 i1="30" i2="3" l="ENG"><s0>Indium additions</s0><s5>42</s5></fC03><fC03 i1="31" i2="3" l="FRE"><s0>FeAs</s0><s4>INC</s4><s5>46</s5></fC03><fC03 i1="32" i2="3" l="FRE"><s0>6166</s0><s4>INC</s4><s5>71</s5></fC03><fC03 i1="33" i2="3" l="FRE"><s0>6150A</s0><s4>INC</s4><s5>72</s5></fC03><fN21><s1>294</s1></fN21><fN44 i1="01"><s1>OTO</s1></fN44><fN82><s1>OTO</s1></fN82></pA></standard></inist></record>Pour manipuler ce document sous Unix (Dilib)
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